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Academic Year: | 2016/7 |
Owning Department/School: | Department of Chemistry |
Credits: | 3 [equivalent to 6 CATS credits] |
Notional Study Hours: | 60 |
Level: | Masters UG & PG (FHEQ level 7) |
Period: |
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Assessment Summary: | EX 100% |
Assessment Detail: |
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Supplementary Assessment: |
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Requisites: |
Before taking this module you must take CH20147 OR take CH20148
In taking this module you cannot take CH40131 |
Description: | Aims: To describe and give examples of some modern techniques for investigating the structure of a range of inorganic molecules. Learning Outcomes: After studying the Unit, students should be able to: * Describe the physical basis, limitations and information available from structural methods, namely, X-Ray crystallography and NMR spectroscopy. * Solve a range of problems by critically assessing numerical and spectroscopic information * Solve problems using the techniques introduced including the application of techniques to unseen situations. Skills: Problem solving (T, F, A), Scientific writing (F, A), Independent working (F), Group working (F). Content: Brief introduction to crystallography. Crystal systems and lattices. Unit cells. Periodicity in lattices. Space group diagrams. Data collection procedures and solving crystal structures. Atomic scattering factors and structure factors. R factors. Theoretical basis of NMR spectroscopy. Spin-spin coupling and chemical shifts in NMR spectroscopy and the factors that affect them. Spin systems. First and second-order spectra. Isotopomers. NMR timescales and static and dynamic NMR spectra. Structural elucidation. |
Programme availability: |
CH40155 is Compulsory on the following programmes:Department of Chemistry
CH40155 is Optional on the following programmes:Programmes in Natural Sciences
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Notes:
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